HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 21469848, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Hydroxybenzophenone | HCID 14347 | — |
| Reactant | 1-Bromo-4-chlorobutane | HCID 81364 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 21469848 | HCID 21469848 | — |
Reaction Steps
Combine 4-hydroxybenzophenone (8 kg, 57,6 mol), potassium carbonate (8 kg, 57.6 mol), and 1-bromo-4-chlorobutane (8.384 kg, 48.9 mol) in acetone (40 L). Heat to reflux. After 20 hours, cool the reaction mixture and filter. Rinse the filter cake with acetone and evaporate the filtrate in vacuo to obtain 4-(4-chlorobutoxy) benzophenone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05691384 |
| Source dataset | uspto-grants-1997_11 |
| ORD ID | ord-e6f2ee4925214997bb90652433800a5e |
| Source note | uspto-grants-1997_11 |