Picric Acid → HCID 3034482, compound

HRID 2295242Notes

Reaction equation

HRID 2295242 reaction equation
[C:1]1([C:15](O)=[C:11]([N+]([O-])=O)[CH:10]=[C:6]([N+:7]([O-])=O)[CH:5]=1)[N+]([O-])=O.[N+]([C:20]1C=CC=CC=1)([O-])=O.[CH2:26](C(C)=O)[CH:27]([CH3:29])[CH3:28]>[Fe]>[CH3:26][C:27]([CH2:29][CH2:10][CH2:11][CH2:15][CH2:1][CH2:5][CH2:6][NH2:7])([CH3:20])[CH3:28]

Participants

5

Reactant 3

HCID 6954Picric AcidHCID 7416NitrobenzeneHCID 7909Methyl Isobutyl Ketone

Product 1

HCID 3034482HCID 3034482, compound

Reagents, catalysts & solvents 1

HCID 23925IronCatalyst

Procedure

Dissolve the picric acid in the methyl isobutyl ketone; add the N-butyl alcohol and elemental iron. The reaction time during stirring is 24 hours. Add the kerosene, nitrobenzene, and Primene.

Sources & evidence

ORD record
ord-1cc6920bdb3d45f78940f0610fd7add6
Source dataset
uspto-grants-1984_01
Patent number
US04424063

Reaction notes

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