Decanoyl chloride → HCID 178443442, compound

HRID 2295344Notes

Reaction equation

Cl.[CH3:2][C:3]1[NH:8][C:7]2[CH:9]=[N:10][CH:11]=[CH:12][C:6]=2[NH:5][N:4]=1.[C:13]([Cl:24])(=[O:23])[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22]>>[ClH:24].[C:13]([N:5]1[C:6]2[CH:12]=[CH:11][N:10]=[CH:9][C:7]=2[NH:8][C:3]([CH3:2])=[N:4]1)(=[O:23])[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22]

Participants

Reactant 2

HCID 66982Decanoyl chloride

HCID 178433915HCID 178433915, compound

Product 1

HCID 178443442HCID 178443442, compoundYield 62.7%

Procedure

3.7 g (0.02 moles) of 3-methyl-1,4-dihydropyrido[3,4-e]-as-triazine hydrochloride are reacted with an excess of caprinic acid chloride as described in Example 2, to obtain 1-caprinoyl-3-methyl-1,4-dihydropyrido[3,4-e]-as-triazine hydrochloride with a yield of 62.7%; m.p.: 237°-238° C.

Sources & evidence

ORD record: ord-9f36313180d440f2a4c3d91a7a6bf582
Source dataset: uspto-grants-1984_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04424351

Reaction notes

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