Cinnamoylbenzene → HCID 3798265, compound

HRID 2295473Notes

Reaction equation

HRID 2295473 reaction equation
[CH:1](=[CH:8][C:9]([C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:17]1([NH:23][NH2:24])[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>C(O)C>[C:17]1([N:23]2[CH:9]([C:11]3[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=3)[CH:8]=[C:1]([C:2]3[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=3)[NH:24]2)[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1

Participants

4

Reactant 2

HCID 7189CinnamoylbenzeneHCID 7516Phenylhydrazine

Product 1

HCID 3798265HCID 3798265, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

20.8 g benzylideneacetophenone was condensed with 10.8 g phenylhydrazine in 400 ml boiling ethanol over 5 hours, and then allowed to cool. During the cooling process the desired reaction product separates. The sediment was filtered, washed with ethanol and dried.

Workup

  1. customover 5 hours
  2. temperatureto cool
  3. customreaction product
  4. filtrationThe sediment was filtered
  5. washwashed with ethanol
  6. customdried

Sources & evidence

ORD record
ord-d52816a7584c405f995ea4670740be4f
Source dataset
uspto-grants-1984_01
Patent number
US04425179

Reaction notes

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