Phenylhydrazine → HCID 67561852, compound

HRID 2295474Notes

Reaction equation

HRID 2295474 reaction equation
[CH:1]1[CH:6]=[CH:5][C:4](/[CH:7]=[CH:8]/[CH:9]=O)=[CH:3][CH:2]=1.[C:11]1([NH:17][NH2:18])[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1>C(O)(=O)C>[C:11]1([N:17]2[CH:7]([C:4]3[CH:5]=[CH:6][CH:1]=[CH:2][CH:3]=3)[CH:8]=[CH:9][NH:18]2)[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

Participants

4

Reactant 2

HCID 7516PhenylhydrazineHCID 637511Cinnamaldehyde

Product 1

HCID 67561852HCID 67561852, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

13.2 g Zimtaldehyde (cinnamaldehyde) was condensed with 10.8 g Phenylhydrazine in 300 ml boiling acetic acid over 2 hours. At room temperature the sediment was filtered, washed with ethanol and dried.

Workup

  1. customover 2 hours
  2. filtrationAt room temperature the sediment was filtered
  3. washwashed with ethanol
  4. customdried

Sources & evidence

ORD record
ord-01b5e719ca134f629599c5d3eb47cadd
Source dataset
uspto-grants-1984_01
Patent number
US04425179

Reaction notes

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