palladium(II) acetate → palladium(II) acetate

HRID 2295477Notes

Reaction equation

HRID 2295477 reaction equation
[C:1]([O-:4])(=[O:3])[CH3:2].[Pd+2:5].[C:6]([O-:9])(=[O:8])[CH3:7]>C(O)(=O)CC>[Pd:5].[C:1]([O-:4])(=[O:3])[CH3:2].[Pd+2:5].[C:6]([O-:9])(=[O:8])[CH3:7]

Participants

4

Reactant 1

HCID 167845palladium(II) acetate

Product 2

HCID 23938PalladiumHCID 167845palladium(II) acetateYield 48%

Reagents, catalysts & solvents 1

HCID 1032Propionic AcidSolvent

Procedure

Granular active carbon of 16 to 32-mesh particle size weighing 10 g was placed in a solution of 760 mg of palladium acetate in 65 ml of propionic acid, and allowed to stand at room temperature for 12 hours. Thereupon, the material was filtered and dried at room temperature in a vacuum desiccator, to finally form a palladium-bearing solid catalyst, about 48% of palladium acetate having been adsorbed on the active carbon.

Workup

  1. filtrationThereupon, the material was filtered
  2. customdried at room temperature in a vacuum desiccator

Sources & evidence

ORD record
ord-86ce32acdd2b4237b740a8125e4a0e55
Source dataset
uspto-grants-1984_01
Patent number
US04425277

Reaction notes

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