HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glutaric anhydride → HCID 15590830, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glutaric anhydride | HCID 7940 | — |
| Reactant | HCID 20474677 | HCID 20474677 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 15590830 | HCID 15590830 | — |
Reaction Steps
113 g (0.396 mol) of 3-(2-benzylaminoethyl)-5-chloroindole are dissolved in 500 ml of benzene. 45.27 g of glutaric anhydride are added in small amounts and the reaction mixture is heated at the reflux temperature for 2 hours and then left to stand overnight. It is evaporated to dryness. This gives the named product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04425351 |
| Source dataset | uspto-grants-1984_01 |
| ORD ID | ord-0884a675153b4c7384afec2345421235 |
| Source note | uspto-grants-1984_01 |