HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13245938, compound → 3-Amino-2-methylphenylmethyl acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13245938 | HCID 13245938 | — |
| Catalyst | Palladium monoxide | HCID 5083724 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-Amino-2-methylphenylmethyl acetate | HCID 13245939 | 97.6% |
Reaction Steps
Using a Parr hydrogenator, 30.0 g (0.143 mol) of 2-methyl-3-nitrophenylmethyl acetate in 250 mL of methanol was hydrogenated in the presence of 0.5 g of palladium oxide on charcoal to give 25.0 g of 3-amino-2-methylphenylmethyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04426524 |
| Source dataset | uspto-grants-1984_01 |
| ORD ID | ord-090f8b7257e2476daa512f9ec917b9f2 |
| Source note | uspto-grants-1984_01 |