HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 13336598, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 13336583 | HCID 13336583 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 13336598 | HCID 13336598 | 47% |
Reaction Steps
A solution of 5-chloro-2-(3-dimethylaminophenoxy)pyrimidine (3.75 g) and methyl iodide (4.50 g) in ether (25 ml) was stirred at room temperature for one week. Filtration of the ether solution gave 2.75 g (47%) of the title compound, mp 155° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04427437 |
| Source dataset | uspto-grants-1984_01 |
| ORD ID | ord-0a99986422ab4ae38529718c07c0ac99 |
| Source note | uspto-grants-1984_01 |