Dimethylcarbamoyl Chloride → HCID 86739196, compound

HRID 2296036Notes

Reaction equation

[N:1](=[C:3]1[C:8]([CH3:9])=[N:7][CH2:6][CH2:5][S:4]1)[OH:2].[CH3:10][N:11]([CH3:15])[C:12](Cl)=[O:13]>>[CH3:10][N:11]([CH3:15])[C:12]([O:2][N:1]=[C:3]1[C:8]([CH3:9])=[N:7][CH2:6][CH2:5][S:4]1)=[O:13]

Participants

Reactant 2

HCID 6598Dimethylcarbamoyl Chloride

HCID 136229043HCID 136229043, compound

Product 1

HCID 86739196HCID 86739196, compound

Procedure

2-Oxo-5,6-dihydro-3-methyl-2H-1,4-thiazine oxime is reacted with dimethylcarbamoyl chloride as described in Example 2 to yield 2-oxo-5,6-dihydro-3-methyl-2H-1,4-thiazine O-(dimethylcarbamoyl) oxime, m.p. 64°-65° C.

Sources & evidence

ORD record: ord-f4c7fda558884977a8150bf048281486
Source dataset: uspto-grants-1984_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04427687

Reaction notes

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