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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2296056Generated: November 1, 2026

Vanillin → N,N-diethyl-m-toluamide

https://huagongshe.com/reaction/2296056

Reaction equation

Participants

RoleNameHCIDCharge
ReactantVanillinHCID 1183—
ReactantHCID 131713373HCID 131713373—
SolventEthanolHCID 702—
ProductVanillinHCID 1183—
ProductN,N-diethyl-m-toluamideHCID 428450%

Reaction Steps

Forestry workers from the Canadian Forestry Service have tested the effects of vanillin-DEET mixtures under field conditions in Northern Ontario. Vanillin was dissolved in ethanol at a concentration of 5 g. vanillin per ml. and this concentrate then added to a commercial repellent containing 47.5% DEET to give a final solution concentration of about 10% vanillin and about 50% DEET. This combined formulation was tested by 25 subjects over extended periods under various conditions (in comparison with the commercial 48% DEET repellent). The comparison was based on both landings and bites. Twenty three out of the 25 subjects reported that the test mixture was a more effective repellent.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04427700
Source datasetuspto-grants-1984_01
ORD IDord-9cf9f7134d554bc08c410b393891fac7
Source noteuspto-grants-1984_01