HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23048576, compound → HCID 20472082, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23048576 | HCID 23048576 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 20472082 | HCID 20472082 | 94.1% |
Reaction Steps
5.6 g of potassium tert.butylate are refluxed for 60 minutes with 6.8 g of 3,4-dimethyladiponitrile in 50 ml of toluene. The cooled solution is washed with 50 ml of water and concentrated. There are obtained 6.4 g (94%) of 2-cyano-3,4-dimethyl-cyclopent-1-enylamine of melting point 92°-100° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04428886 |
| Source dataset | uspto-grants-1984_01 |
| ORD ID | ord-562c1bbe62104d11b2ed7b6247ba9656 |
| Source note | uspto-grants-1984_01 |