HCID 13247952, compound → Diisopropylaniline

HRID 2296505Notes

Reaction equation

HRID 2296505 reaction equation
[CH:1]([CH:4]1[CH2:9][CH2:8][CH2:7][CH:6]([CH:10]([CH3:12])[CH3:11])[CH:5]1[NH2:13])([CH3:3])[CH3:2]>[Pd]>[CH:10]([C:6]1[CH:7]=[CH:8][CH:9]=[C:4]([CH:1]([CH3:3])[CH3:2])[C:5]=1[NH2:13])([CH3:12])[CH3:11]

Participants

3

Reactant 1

HCID 13247952HCID 13247952, compound

Product 1

HCID 32484DiisopropylanilineYield 93%

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

The procedure described in Example 27 is followed, using a catalyst which contains 1.0% by weight of palladium on a zinc/aluminum spinel and starting from 2,6-diisopropylcyclohexylamine. 2,6-Diisopropylaniline (boiling point=257° C.) is obtained in a yield of 93% of the theory.

Sources & evidence

ORD record
ord-a09644891afd483a98993050be61c4fe
Source dataset
uspto-grants-1984_01
Patent number
US04429155

Reaction notes

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