HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 9794302, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | Diazabicyclooctane | HCID 66583054 | — |
| Product | HCID 9794302 | HCID 9794302 | — |
Reaction Steps
The product of Example 31d is treated with oxalyl chloride and diazabicyclooctane in acetonitrile to give the title compound, which is purified by partition between water and EtOAc, and passage over a silica column.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06489323B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-8285ccbb61d143f2b6bc070661e62185 |
| Source note | uspto-grants-2002_12 |