Acetonitrile → HCID 9794302, Verbindung

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Reaktionsgleichung

[C:1](Cl)(=[O:5])[C:2](Cl)=[O:3].[N:7]1([CH:15]2[CH2:22][CH2:21][CH2:20][CH2:19][CH2:18][CH2:17][CH2:16]2)[CH2:14]CCCCCN1.C(#[N:25])C>>[CH2:22]([CH:15]1[N:7]2[C:1](=[O:5])[C:2](=[O:3])[N:25]=[C:14]2[CH2:17][CH2:16]1)[CH2:21][CH2:20][CH2:19][CH3:18]

Komponenten

Edukt 3

HCID 6342Acetonitrile

HCID 65578Oxalyl chloride

HCID 66583054Diazabicyclooctane

Produkt 1

HCID 9794302HCID 9794302, Verbindung

Versuchsvorschrift

The product of Example 31d is treated with oxalyl chloride and diazabicyclooctane in acetonitrile to give the title compound, which is purified by partition between water and EtOAc, and passage over a silica column.

Quellen und Nachweise

ORD-Eintrag: ord-8285ccbb61d143f2b6bc070661e62185
Quelldatensatz: uspto-grants-2002_12
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US06489323B1

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