HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium ethoxide → HCID 23500526, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium ethoxide | HCID 2723922 | — |
| Reactant | HCID 9837766 | HCID 9837766 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23500526 | HCID 23500526 | — |
Reaction Steps
To the product of Example 37a or the product of Example 15 in ethanol is added an ethanolic solution of sodium ethoxide. After thin layer chromatography indicates the reaction is complete, it is concentrated and the residue partitioned between water and an extraction solvent. The dried organic layer is stripped of all solvent and the residue chromatographed to produce the title material.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06489323B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-e525b59fe7f4479c84e13a9fc69f33ff |
| Source note | uspto-grants-2002_12 |