HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 56987812, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 54107311 | HCID 54107311 | — |
| Reactant | HCID 86755963 | HCID 86755963 | — |
| Product | HCID 56987812 | HCID 56987812 | — |
Reaction Steps
The title compound was prepared in a manner similar to the product of Example 11 except that cesium carbonate/lithium iodide rather than sodium hydride was used in the final reaction step: mp 169-170°; HRMS: Calcd. for C18H14NO3F3Cl (M+H)+: 384.061431. Found: 384.058632.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06489320B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-2786be2bf8a44cc6b59f1c9cfb733795 |
| Source note | uspto-grants-2002_12 |