Methanol → HCID 70077352, compound

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Reaction Steps

A 6.6N NaOH solution (0.5 ml) was added to a mixture of Compound 30 as prepared in Example 17 (0.05 g, 0.096 mM) in methanol. The mixture was stirred at reflux overnight, cooled to room temperature and evaporated in vacuo. The residue was diluted with water and enough 6N HCl was added drop-wise to precipitate the product. The solid product was collected by filtration and dried. m/z (MH+)537

Provenance & Evidence