HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylbenzoyl chloride → HCID 18387444, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylbenzoyl chloride | HCID 70276 | — |
| Reactant | [1,1'-Biphenyl]-2-carbonyl chloride | HCID 12563768 | — |
| Reactant | HCID 18387440 | HCID 18387440 | — |
| Product | HCID 18387444 | HCID 18387444 | 64% |
Reaction Steps
2-(2-Hydroxyethyl)-5-(4-aminobenzyl)-1,5-benzothiazepine-4-one as prepared in Example 21 (0.105 g, 0.31 mM) was treated using the procedure described in Example 22, with o-toluoyl chloride (0.04 ml, 0.33 mM) substituted for 2-phenylbenzoyl chloride, to yield the title product as a white solid (0.086 g, 64%) m/z (MH+) 447
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06489321B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-0e4cd01fe50a465886d393c0bdc029c0 |
| Source note | uspto-grants-2002_12 |