HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → HCID 18387446, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 18387431 | HCID 18387431 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 18387446 | HCID 18387446 | — |
Reaction Steps
Methanesulfonyl chloride (0.04 ml, 0.55 mM) was added to Compound 23 as prepared in Example 22 (0.280 g, 0.55 mM) and triethylamine (0.15 ml, 1.1 mM) following the procedure described in Example 29 to give the solid product. m/z (MH+) 587.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06489321B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-167bef7bac0f4dd1a67def772b7a1a00 |
| Source note | uspto-grants-2002_12 |