Azobisisobutyronitrile → HCID 86583984, compound

Participants

Reaction Conditions

Reaction Steps

To a 500 ml round-bottom flask was added 0.3 mole of 9-anthracenemethylacrylate, 0.5 mole of 4-hydroxybutylacrylate, 0.2 mole of methylmethacrylate, 300 g of THF, and 0.1-3 g of AIBN. The resulting solution was stirred at 60-75° C. for 5-20 hours under nitrogen atmosphere. The reaction mixture was precipitated in ethyl ether or n-hexane. The precipitate was filtered and dried to provide poly[9-anthracenemethylacrylate/4-hydroxybutylacrylate/methylmethacrylate] copolymer of Formula 21. Yield: 81%.

Provenance & Evidence