Potassium Carbonate → HCID 23511466, compound

HRID 2297013Notes

Reaction equation

HRID 2297013 reaction equation
C([O:4][CH2:5][CH2:6][CH:7]([C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][N:13]=1)[O:8]C(=O)C)(=O)C.C(=O)([O-])[O-].[K+].[K+]>CO.O>[N:13]1[CH:14]=[CH:15][CH:16]=[CH:17][C:12]=1[CH:7]([OH:8])[CH2:6][CH2:5][OH:4]

Participants

4

Reactant 2

HCID 11430Potassium CarbonateHCID 265145HCID 265145, compound

Product 1

HCID 23511466HCID 23511466, compound

Reagents, catalysts & solvents 1

HCID 22242641Methanol--water (1/1)Solvent

Procedure

A solution of 3-(2-pyridyl)-1,3-propanediol diacetate (1 mmole) in methanol-water (3:1) was treated with potassium carbonate (5 mmole) at 25° C. for 3 h. Evaporation and chromatography gave 3-(2-pyridyl)-1,3-propanediol as a solid.

Workup

  1. customEvaporation and chromatography

Sources & evidence

ORD record
ord-643f0f2d7a44432e840191bb117d5bd2
Source dataset
uspto-grants-2002_12
Patent number
US06489476B1

Reaction notes

Loading…