HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Tert-Butylphenol → Cyclohexanol, 2-(1,1-dimethylethyl)-, (1R,2R)-rel-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Tert-Butylphenol | HCID 6923 | — |
| Reactant | 2-tert-Butylcyclohexyl acetate | HCID 62334 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Product | Cyclohexanol, 2-(1,1-dimethylethyl)-, (1R,2R)-rel- | HCID 6995536 | — |
Reaction Steps
A pressurized container fitted with stirrer is charged with 2-tertiary-butylphenol, 2-tertiary-butylcyclohexyl acetate and the catalyst. Hydrogenation is carried out at the chosen reaction temperature and hydrogen pressure. The resulting cis-2-tertiary-butylcyclohexanol is obtained following removal of the catalyst by filtration, decantation or centrifugation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06489520B2 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-5d06102f987e48c39d6f408953fbfe37 |
| Source note | uspto-grants-2002_12 |