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HRID2297143

反应详情

EQUATION

反应方程式

HRID 2297143 的结构方程式

REACTANTS

反应物

2
结构：COC(OC)N(C)C
HCID78373

Methanamine, 1,1-dimethoxy-N,N-dimethyl-

C5H13NO2

结构：CCc1ccc(C(=O)Cc2ncc[nH]2)cc1
HCID22142578

未命名化合物

PRODUCTS

生成物

1
结构：CCc1ccc(C(=O)/C(=C/N(C)C)c2ncc[nH]2)cc1
HCID22142876

未命名化合物

PROCEDURE

实验过程

1 mmol of 1-(4-ethylphenyl)-2-imidazolylethan-1-one was heated to 80° C. in N,N-dimethylformamidedimethyl acetal for six hours and concentrated in vacuo to obtain (2E)-3-(dimethylamino)-1-(4-ethylphenyl)-2-imidazolylprop-2-en-1-one.

WORKUP

后处理

  1. concentrationconcentrated in vacuo