HRID229745

反应详情

EQUATION

反应方程式

HRID 229745 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

26 g of benzophenone imine are added to 34 g of 5-bromo-1,3-thiazol-2-amine hydrobromide, in suspension in 300 ml of 1,2-dichloroethane. The mixture is kept under reflux for 18 hours. The precipitate formed is filtered and the filtrate is concentrated to give 37.2 g of solid.

WORKUP

后处理

  1. temperatureunder reflux for 18 hours
  2. customThe precipitate formed
  3. filtrationis filtered
  4. concentrationthe filtrate is concentrated