HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Phenylenediamine → HCID 178500070, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Phenylenediamine | HCID 7243 | — |
| Reactant | Dimethyl alpha-ketoglutarate | HCID 25775 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178500070 | HCID 178500070 | 101.2% |
Reaction Steps
Dimethyl 2-ketoglutarate (3.75 g) and o-phenylenediamine (2.5 g) were dissolved in methanol (30 ml), and the mixture was stirred overnight. The precipitated crystals were recovered by filtration and washed with water and methanol to obtain 5.06 g of methyl 3-(3-hydroxyquinoxaline-2-yl)propanoate Yield: 94%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06492364B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-1ecbb4076d184381b57f51e787aa11c2 |
| Source note | uspto-grants-2002_12 |