Methyl chloroformate → methyl N-[4-[4-(6-chloronaphthalen-2-yl)sulfonylpiperazine-1-carbonyl]benzenecarboximidoyl]carbamate

Participants

Role	Name	HCID	Charge
Reactant	Methyl chloroformate	HCID 6586	—
Reactant	4-[4-(6-Chloro-2-naphthylsulphonyl)piperazine-1-carbonyl]-3-methylbenzamidine	HCID 18382293	—
Solvent	Dichloromethane	HCID 6344	—
Product	methyl N-[4-[4-(6-chloronaphthalen-2-yl)sulfonylpiperazine-1-carbonyl]benzenecarboximidoyl]carbamate	HCID 145840733	—

Reaction Steps

By reaction of 4-[4-(6-chloro-2-naphthylsulphonyl)piperazine-1-carbonyl]-3-methylbenzamidine with methyl chloroformate in dichloromethane, the compound methyl(imino-{4-[4- (6-chloro-2-naphthylsulphonyl)piperazine-1-carbonyl]phenyl}methyl)carbamate is obtained after customary work-up

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US06492368B1
Source dataset	uspto-grants-2002_12
ORD ID	ord-6d0f007a0da6494e98a9989bf4a06818
Source note	uspto-grants-2002_12