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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2297673Generated: October 30, 2026

Hydroxylamine → HCID 86588181, compound

https://huagongshe.com/reaction/2297673

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydroxylamineHCID 787—
ReactantHCID 69827849HCID 69827849—
SolventEthanolHCID 702—
ProductHCID 86588181HCID 86588181—

Reaction Conditions

Temperature22 °C

Reaction Steps

A mixture of 1-[(3aR,4R,6R,6aR)-6-methoxy-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl]pent-1-yn-3-one (550 mg) and hydroxylamine (50% solution in water) (0.2 ml) in ethanol (10 ml) was stirred overnight at 22° C. The mixture was concentrated in vacuo to afford the title compound as a yellow oil (554 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06492348B1
Source datasetuspto-grants-2002_12
ORD IDord-db5b6b9db0bf4d5e830eb2e26e99a472
Source noteuspto-grants-2002_12