Hydrogen Peroxide → HCID 18383971, compound

Participants

Reaction Steps

A mixture of 2.5 g (0.0074 mole) of 2-chloro-1-[1-methyl-5-(4-(methylsulfinyl)benzoyl]-1H-pyrrol-3-yl]-ethanone, 20 mL of HOAc, and 1.7 mL of 30% H2O2 was stirred for 6 days. The solid was filtered off to give 0.75 g (30%) of 2-chloro-1-[1-methyl-5-(4-(methylsulfonyl)benzoyl]-1H-pyrrol-3-yl]-ethanone. HNMR (CDCl3) δ8.1 (s, 2H); 8.0 (s, 2H); 7.7 (ar, 1H); 7.1 (ar, 1H); 4.4 (s, 2H); 4.1 (s, 3H); 3.1 (s, 3H).

Provenance & Evidence