N,N-Dimethylethylenediamine → HCID 18382953, compound

HRID 2297768Notes

Reaction equation

HRID 2297768 reaction equation
[CH3:1][N:2]([CH3:6])[CH2:3][CH2:4][NH2:5].[NH:7]1[C:15]2[C:10](=[CH:11][C:12]([NH:16][C:17]3[C:18]4[S:25][C:24]([C:26]5[CH:33]=[CH:32][C:29]([CH:30]=O)=[CH:28][CH:27]=5)=[CH:23][C:19]=4[N:20]=[CH:21][N:22]=3)=[CH:13][CH:14]=2)[CH:9]=[CH:8]1>>[NH:7]1[C:15]2[C:10](=[CH:11][C:12]([NH:16][C:17]3[C:18]4[S:25][C:24]([C:26]5[CH:33]=[CH:32][C:29]([CH2:30][NH:5][CH2:4][CH2:3][N:2]([CH3:6])[CH3:1])=[CH:28][CH:27]=5)=[CH:23][C:19]=4[N:20]=[CH:21][N:22]=3)=[CH:13][CH:14]=2)[CH:9]=[CH:8]1

Participants

3

Reactant 2

HCID 66053N,N-DimethylethylenediamineHCID 183827594-(4-(1H-indol-5-ylamino)-thieno[3,2-d]pyrimidin-6-yl]-benzaldehyde

Product 1

HCID 18382953HCID 18382953, compound

Procedure

The title compound was prepared from N,N-dimethylethylenediamine and 4-[4-(1H-indol-5-ylamino)-thieno[3,2-d]pyrimidin-6-yl]-benzaldehyde by a procedure analogous to example 17. M.P. 170-183° C.; LC-MS: 443 (MH+); HPLC RT: 3.02 minutes.

Sources & evidence

ORD record
ord-496669695bb947de90a9c3445e526cb3
Source dataset
uspto-grants-2002_12
Patent number
US06492383B1

Reaction notes

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