HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Methylthio)phenylboronic acid → (1H-Indol-5-yl)-[2-(4-methylsulfanyl-phenyl)-thieno[3,2-b]pyridin-7-yl]-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Methylthio)phenylboronic acid | HCID 2733959 | — |
| Reactant | (2-bromo-thieno[3,2-b]pyridin-7-yl)-(1H-indol-5-yl)-amine | HCID 18382766 | — |
| Product | (1H-Indol-5-yl)-[2-(4-methylsulfanyl-phenyl)-thieno[3,2-b]pyridin-7-yl]-amine | HCID 9865061 | — |
Reaction Steps
The title compound was prepared from 4-(methylthio)benzeneboronic acid and (2-bromo-thieno[3,2-b]pyridin-7-yl)-(1H-indol-5-yl)-amine by a procedure analogous to example 17. 1H NMR (400 MHz, DMSO) d 11.4 (s, 1H), 10.6 (s, 1H), 8.30 (d, 1H), 7.53 (m, 9H), 7.05 (d, 1H), 6.43 (s, 1H), 2.48 (s, 3H); LC-MS: 388 (MH+); HPLC RT: 6.07 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06492383B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-688f0a89971b4783af75e444c95b8283 |
| Source note | uspto-grants-2002_12 |