HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-(Diethylamino)-2-benzofurancarboxaldehyde → 1-(5-carboxy-pentyl)-4-[(E)-2-(6-diethylamino-benzofuran-2-yl)-vinyl]-6-sulfonato-chinolinium betaine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-(Diethylamino)-2-benzofurancarboxaldehyde | HCID 14716710 | — |
| Reactant | 1-(5-Carboxy-pentyl)-4-methyl-6-sulfonato-chinolinium betaine | HCID 131727539 | — |
| Solvent | Methanol--water (1/1) | HCID 22242641 | — |
| Product | 1-(5-carboxy-pentyl)-4-[(E)-2-(6-diethylamino-benzofuran-2-yl)-vinyl]-6-sulfonato-chinolinium betaine | HCID 131727540 | — |
Reaction Steps
0.2 mmol 6-diethylamino-benzofuran-2-carbaldehyde and 0.2 mmol 1-(5-carboxy-pentyl)-4-methyl-6-sulfonato-chinolinium betaine are converted according to the general directions given above. Column chromatography: SiO2 (RP18), eluent: methanol/water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07563907B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-b547ae899ff64f9997e290c94269ff67 |
| Source note | uspto-grants-2009_07 |