HuagongsheHuagongshe Chemistry Print Report · For research reference only
(5-Methylthiophen-2-yl)boronic acid → HCID 18382838, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (5-Methylthiophen-2-yl)boronic acid | HCID 2734374 | — |
| Reactant | 2-Bromo-N-(2-methyl-1H-indol-5-yl)thieno[3,2-b]pyridin-7-amine | HCID 18382850 | — |
| Product | HCID 18382838 | HCID 18382838 | — |
Reaction Steps
The title compound was prepared from 5-methylthiophene-2-boronic acid and (2-bromothieno[3,2-b]pyridin-7-yl)-(2-methyl-1H-indol-5-yl)-amine by the procedure analogous to example 2 above. 1H NMR (400 MHz, CD3OD) δ8.03 (d, 1H), 7.29 (m, 3H), 7.15 (s, 1H), 6.99 (m, 1H), 6.83 (d, 1H), 6.54 (d, 1H), 6.10 (s, 1H), 2.41 (s, 3H), 2.22 (s, 3H); RP18-HPLC RT: 6.08 minutes; API MS: 376 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06492383B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-ab012cf6015443e0a13db80f210c3ed7 |
| Source note | uspto-grants-2002_12 |