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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2297847Generated: November 1, 2026

5-Amino-2-methylindole → HCID 18383063, compound

https://huagongshe.com/reaction/2297847

Reaction equation

Participants

RoleNameHCIDCharge
Reactant5-Amino-2-methylindoleHCID 2733992—
ReactantHCID 18382752HCID 18382752—
ProductHCID 18383063HCID 18383063—

Reaction Steps

The title compound was prepared from 2-methyl-5-aminoindole and 7-chloro-2-[6-(2,5-dimethyl-pyrrol-1-yl)-2-methyl-pyridin-3-yl]-thieno[3,2-b]pyridine by the procedure analogous to example 148(c) above. 1H NMR (400 MHz, CD3OD) δ8.08 (s, 1H), 7.82 (d, 1H), 7.40 (s, 1H), 7.30 (s, 1H), 7.25 (d, 1H), 7.07 (d, 1H), 6.92 (dd, 1H), 6.58 (d, 1H), 6.07 (s, 1H), 5.80 (s, 2H), 2.60 (s, 3H), 2.36 (s, 3H), 2.05 (s, 6H); RP18-HPLC RT: 6.55 minutes; API MS: 464 (M+1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06492383B1
Source datasetuspto-grants-2002_12
ORD IDord-2dfe9f6558824c1fbf9ff40e03c09636
Source noteuspto-grants-2002_12