HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2298031Generated: October 30, 2026
HCID 11133523, compound → HCID 11058459, compound
https://huagongshe.com/reaction/2298031
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 11133523 | HCID 11133523 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 11058459 | HCID 11058459 | 74% |
Reaction Steps
The product of step b) (2.63 g, 6.29 mmol) was suspended in acetic acid (30.0 ml) and heated to 110° C. until all the starting material has been consumed after about 3 hours. The solvent was removed and the residue titurated with diethyl ether to give the sub-title compound (1.84 g, 74%) as an off-white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06492409B1 |
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| Source dataset | uspto-grants-2002_12 |
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| ORD ID | ord-cab3fe286bd94e82ab62acb6db397b0b |
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| Source note | uspto-grants-2002_12 |
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