HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tricyclo(3.3.1.13,7)dec-1-ylmethylamine → HCID 57244288, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tricyclo(3.3.1.13,7)dec-1-ylmethylamine | HCID 86625 | — |
| Reactant | HCID 18381485 | HCID 18381485 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 57244288 | HCID 57244288 | — |
Reaction Steps
Prepared as described in Example 5c) using 2-chloro-5-[4-[[(1,1-dimethylethoxy)carbonyl]amino]-1-piperidinyl]-benzoic acid (Example 6b, 0.065 g), N,N′-carbonyldiimidazole (0.030 g), 1-adamantanemethylamine (0.032 ml) and dimethylformamide (3 ml) to give the subtitle compound as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06492355B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-2db6b50840344e5c8f15fe2ba3f58572 |
| Source note | uspto-grants-2002_12 |