HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tricyclo(3.3.1.13,7)dec-1-ylmethylamine → HCID 57037521, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tricyclo(3.3.1.13,7)dec-1-ylmethylamine | HCID 86625 | — |
| Reactant | HCID 53742797 | HCID 53742797 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 57037521 | HCID 57037521 | — |
Reaction Steps
Prepared as described in Example 5c) using (+/−)-2-chloro-5-[3-[[(1,1-dimethylethoxy)carbonyl]amino]-1-pyrrolidinyl]-benzoic acid (Example 7b, 0.070 g), N,N′-carbonyldiimidazole (0.033 g), 1-adamantanemethylamine (0.036 ml) and dimethylformamide (3 ml) to give the subtitle compound as a gum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06492355B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-a38a354068ad40f08a0a06fefebc0067 |
| Source note | uspto-grants-2002_12 |