HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 54030420, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | 5-Iodosalicylic acid | HCID 8388 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 54030420 | HCID 54030420 | — |
Reaction Steps
5-Iodosalicylic acid (2.0 g, 7.58 mmol) in toluene was treated with SOCl2 (1.66 mL, 22.7 mmol) and catalytic DMF at reflux for 1 h. The reaction mixture was evaporated to dryness and the acid chloride used in the next step without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06492425B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-437be27a1cb44413a30fc9ae62112a26 |
| Source note | uspto-grants-2002_12 |