HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromopropionic acid → Tert-butyl 3-bromopropanoic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromopropionic acid | HCID 11553 | — |
| Reactant | Tert-butyl 6-bromohexanoate | HCID 11550568 | — |
| Solvent | Isobutylene | HCID 8255 | — |
| Product | Tert-butyl 3-bromopropanoic Acid | HCID 18386960 | 36% |
Reaction Steps
3-Bromopropanoic acid (8.2 g, 53.6 mmol) and iso-butene (60 ml) were reacted by the same procedure as described in Example 1 for the preparation of tert-butyl 6-bromohexanoate and afforded the title material (4 g, 36%) as a colorless liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06492550B2 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-a0314a9b9ca7423286f81dccf0377d9b |
| Source note | uspto-grants-2002_12 |