3-Pyridinecarboxaldehyde → HCID 69590587, compound

HRID 2298550Notes

Reaction equation

HRID 2298550 reaction equation
[C:1]([N:5]1[C@@H:9]([CH2:10][C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[CH2:8][O:7][C:6]1=[O:17])(=[O:4])[CH2:2][CH3:3].[N:18]1[CH:23]=[CH:22][CH:21]=[C:20]([CH:24]=[O:25])[CH:19]=1>>[CH3:3][C@@H:2]([C@@H:24]([OH:25])[C:20]1[CH:19]=[N:18][CH:23]=[CH:22][CH:21]=1)[C:1]([N:5]1[C@@H:9]([CH2:10][C:11]2[CH:12]=[CH:13][CH:14]=[CH:15][CH:16]=2)[CH2:8][O:7][C:6]1=[O:17])=[O:4]

Participants

3

Reactant 2

HCID 103713-PyridinecarboxaldehydeHCID 2733696(4S)-4-Benzyl-3-propanoyl-1,3-oxazolidin-2-one

Product 1

HCID 69590587HCID 69590587, compound

Procedure

Prepared from (4S)-N-propionyl-4-benzyl-2-oxazolidinone and pyridine-3-carboxaldehyde according to the procedure described in Example 1, paragraph A. 13C-NMR (100 MHz, CDCl3): δ 176.40, 152.83, 148.74, 147.85, 136.78, 134.80, 134.04, 129.34, 128.95, 127.45, 123.21, 109.75, 71.46, 66.23, 55.05, 44.28, 37.70, 10.64.

Sources & evidence

ORD record
ord-e27e1ca712a84a3a8aea05aac99bd401
Source dataset
uspto-grants-2002_12
Patent number
US06492562B1

Reaction notes

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