HCID 53767114, compound → 5-(3-Amino-1-propenyl)-2-benzoxazolone

HRID 2298565Notes

Reaction equation

HRID 2298565 reaction equation
C(OC([NH:8][CH2:9][CH:10]=[CH:11][C:12]1[CH:13]=[CH:14][C:15]2[O:19][C:18](=[O:20])[NH:17][C:16]=2[CH:21]=1)=O)(C)(C)C>FC(F)(F)C(O)=O>[NH2:8][CH2:9][CH:10]=[CH:11][C:12]1[CH:13]=[CH:14][C:15]2[O:19][C:18](=[O:20])[NH:17][C:16]=2[CH:21]=1

Participants

3

Reactant 1

HCID 53767114HCID 53767114, compound

Product 1

HCID 537395895-(3-Amino-1-propenyl)-2-benzoxazolone

Reagents, catalysts & solvents 1

HCID 6422Trifluoroacetic acidSolvent

Procedure

A solution of 5-(3-(t-butoxycarbonylamino)-1-propenyl)-2-benzoxazolone in trifluoroacetic acid is stirred at ambient temperature for 30 min, then evaporated to dryness to yield 5-(3-amino-1-propenyl)-2-benzoxazolone.

Workup

  1. customevaporated to dryness

Sources & evidence

ORD record
ord-ab036a80c7154ee8b5c8e6607e82946c
Source dataset
uspto-grants-2002_12
Patent number
US06492562B1

Reaction notes

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