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HRID229858

反应详情

EQUATION

反应方程式

HRID 229858 的结构方程式

REACTANTS

反应物

4
结构：COC(=O)CC(C)=O
HCID7757

Methyl acetoacetate

C5H8O3

结构：NN1CCCCC1
HCID16658

N-Aminopiperidine

C5H12N2

结构：COc1cc(C)c(Cl)cc1C(=O)CBr
HCID2756888

2-bromo-1-(5-chloro-2-methoxy-4-methylphenyl)ethanone

C10H10BrClO2

结构：NCC1COCCO1
HCID3748064

1,4-dioxan-2-ylmethanamine

C5H11NO2

PRODUCTS

生成物

1
结构：COc1cc(C)c(Cl)cc1-c1cc(C(=O)NN2CCCCC2)c(C)n1CC1COCCO1
HCID11590743

未命名化合物

PROCEDURE

实验过程

The title compound was synthesized in analogy to Example 7, using 3-oxo-butyric acid methyl ester as compound of formula R, 2-bromo-1-(5-chloro-2-methoxy-4-methyl-phenyl)-ethanone (purchased from Oakwood) as compound of formula S, rac-1,4-dioxane-2-methanamine as R3—(CH2)m—NH2 and piperidine-1-ylamine as R1R2NH, MS (ISP) 462.2 (M+H)+.