HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-1-(3,5-dimethoxyphenyl)ethanone → HCID 86758665, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-1-(3,5-dimethoxyphenyl)ethanone | HCID 2756932 | — |
| Reactant | Methyl 4-(aminothioxomethyl)-5-methylthiothiophene-2-carboxylate | HCID 86583815 | — |
| Product | HCID 86758665 | HCID 86758665 | 27.8% |
Reaction Steps
100 mg (0.404 mmol) of methyl 4-(aminothioxomethyl)-5-methylthiothiophene-2-carboxylate (Maybridge Chemical Co. LTD., Cornwall, U.K.) was reacted with 2-bromo-3′,5′-dimethoxy acetophenone (0.444 mmol) in a manner similar to Example 22, step (a) to afford 44 mg (27% yield) of methyl 4-[4-(3,5-dimethoxyphenyl)(1,3-thiazol-2-yl)]-5-methylthiothiophene-2-carboxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06492403B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-9cb06de0be104090924ed9c0a9a843a0 |
| Source note | uspto-grants-2002_12 |