HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 178433913, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Indole-3-Carboxaldehyde | HCID 10256 | — |
| Reactant | HCID 178429269 | HCID 178429269 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178433913 | HCID 178433913 | — |
Reaction Steps
2.55 g of 5-hydroxy-3-methyl-1-(4-sulfophenyl)-1H-pyrazole, 1.45 g of indole-3-carboxaldehyde and 1.05 g of triethylamine in 25 mL of ethanol were heated at 60° C. After 12 hours, the mixture was cooled, acetone was added dropwise so as to induce crystallization, and the mixture was then filtered.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06494923B2 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-e951cbca74d64d4f9253979b85d145eb |
| Source note | uspto-grants-2002_12 |