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HRID2298699

反应详情

EQUATION

反应方程式

HRID 2298699 的结构方程式

REACTANTS

反应物

3
结构：CC1=NN(c2ccccc2)C(=O)C1
HCID4021

1-Phenyl-3-methyl-5-pyrazolone

C10H10N2O

结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：O=Cc1ccccc1S(=O)(=O)[O-].[Na+]
HCID3794540

Sodium 2-formylbenzenesulfonate

C7H5NaO4S

PRODUCTS

生成物

1
结构：CC1=NN(c2ccccc2)C(=O)C1=Cc1ccccc1S(=O)(=O)[O-].[Na+]
HCID74088227

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

2.1 g of sodium benzaldehyde-2-sulfonate, 1.75 g of 3-methyl-1-phenyl-2-pyrazolin-5-one and 1 g of triethylamine in 20 mL of ethanol were allowed to reflux 5 hours. After cooling to room temperature, the precipitate was filtered off and dried.

WORKUP

后处理

  1. temperatureto reflux 5 hours
  2. filtrationthe precipitate was filtered off
  3. customdried