Ethanol → HCID 86596485, compound

Participants

Reaction Steps

A colorless solid (0.078 g, yield: 82.1%) was obtained through a reaction conducted as in example 2 except that the reactants were replaced by the compound (117) prepared in example 17 (0.1 g), ethanol (66.6 mL), chloroform (100 mL), and sulfuric acid (36 N, 0.3 mL), and the reaction time was adjusted to 96 hours. IR analysis of the product revealed the existence of an absorption band that suggested an acetoxy group at 1740 cm−1. 1H-NMR analysis revealed the product consists of a compound (138) and the compound (117) (content of compound (138): 90.1 mol %).

Provenance & Evidence