HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 70153727, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 57037837 | HCID 57037837 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 70153727 | HCID 70153727 | — |
Reaction Steps
N-[(5S)-3-(3-Fluoro-4-(4-(6-aminopyridin-2-ylaminocarbonyl)imidazol-1-yl)phenyl)-2-oxooxazolidin-5-ylmethyl]acetamide (70 mg, 0.15 mM) was dissolved in pyridine (3 ml) and treated with acetic anhydride (0.5 ml). After standing 60 hours at ambient temperature, solvent was evaporated, and the residue triturated with water (10 ml). Filtration gave the title product (47 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06495551B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-635c0939340e44699a2048bf2c1566de |
| Source note | uspto-grants-2002_12 |