p-Toluenesulfonic acid → HCID 131723719, compound

HRID 2299044Notes

Reaction equation

HRID 2299044 reaction equation
[I:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([NH2:8])=[O:7])=[CH:4][CH:3]=1.[CH3:11][C:12]([CH:15]=O)([CH3:14])[CH3:13].[NH:17]1[C:21]2[CH:22]=[CH:23][CH:24]=[CH:25][C:20]=2[N:19]=[N:18]1.C1(C)C=CC(S(O)(=O)=O)=CC=1>>[N:17]1([CH:15]([C:5]2([CH:9]=[CH:10][C:2]([I:1])=[CH:3][CH2:4]2)[C:6]([NH2:8])=[O:7])[C:12]([CH3:13])([CH3:14])[CH3:11])[C:21]2[CH:22]=[CH:23][CH:24]=[CH:25][C:20]=2[N:19]=[N:18]1

Participants

5

Reactant 4

HCID 6101p-Toluenesulfonic acidHCID 12417PivalaldehydeHCID 775614-IodobenzamideHCID 178418385HCID 178418385, compound

Product 1

HCID 131723719HCID 131723719, compound

Procedure

A suspension of 4-iodobenzamide, pivaldehyde, benzotriazole, and p-toluenesulfonic acid was processed as described in Example IC to provide the title compound.

Sources & evidence

ORD record
ord-fdca3060d088487da787b026105065bd
Source dataset
uspto-grants-2002_12
Patent number
US06495576B2

Reaction notes

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