p-Toluenesulfonic acid → N-[2,2-Bis[(allyloxy)methyl]-1-(1H-1,2,3-benzotriazol-1-yl)butyl]4-chlorobenzamide

HRID 2299057Notes

Reaction equation

HRID 2299057 reaction equation
[CH2:1]([O:4][CH2:5][C:6]([CH2:11][O:12][CH2:13][CH:14]=[CH2:15])([CH2:9][CH3:10])[CH:7]=O)[CH:2]=[CH2:3].[Cl:16][C:17]1[CH:25]=[CH:24][C:20]([C:21]([NH2:23])=[O:22])=[CH:19][CH:18]=1.[NH:26]1[C:30]2[CH:31]=[CH:32][CH:33]=[CH:34][C:29]=2[N:28]=[N:27]1.C1(C)C=CC(S(O)(=O)=O)=CC=1>>[CH2:1]([O:4][CH2:5][C:6]([CH2:11][O:12][CH2:13][CH:14]=[CH2:15])([CH2:9][CH3:10])[CH:7]([NH:23][C:21](=[O:22])[C:20]1[CH:24]=[CH:25][C:17]([Cl:16])=[CH:18][CH:19]=1)[N:26]1[C:30]2[CH:31]=[CH:32][CH:33]=[CH:34][C:29]=2[N:28]=[N:27]1)[CH:2]=[CH2:3]

Participants

5

Reactant 4

HCID 6101p-Toluenesulfonic acidHCID 120844-ChlorobenzamideHCID 183797072,2-Bis[(allyloxy)methyl]butanalHCID 178418385HCID 178418385, compound

Product 1

HCID 18770679N-[2,2-Bis[(allyloxy)methyl]-1-(1H-1,2,3-benzotriazol-1-yl)butyl]4-chlorobenzamide

Procedure

The product from Example 20A, 4-chlorobenzamide, benzotriazole, and p-toluenesulfonic acid were processed as described in Example 1C to provide the title compound.

Sources & evidence

ORD record
ord-618dd6cb3c1c4728866a24b009d134e3
Source dataset
uspto-grants-2002_12
Patent number
US06495576B2

Reaction notes

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