Oxalyl chloride → 28523-30-0

HRID 2299059Notes

Reaction equation

HRID 2299059 reaction equation

[CH:1]1([C:7]([CH3:11])([CH3:10])[CH2:8][OH:9])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.C(Cl)(=O)C(Cl)=O>CS(C)=O>[CH:1]1([C:7]([CH3:11])([CH3:10])[CH:8]=[O:9])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

4

Reactant 2

HCID 65578Oxalyl chloride

HCID 187705282-Cyclohexyl-2-methylpropan-1-ol

Product 1

HCID 1400235028523-30-0

Reagents, catalysts & solvents 1

HCID 679Dimethyl SulfoxideSolvent

Procedure

2-Cyclohexyl-2-methyl-1-propanol, oxalyl chloride and dimethylsulfoxide were processed as described in Example 18A to provide the title compound.

Sources & evidence

ORD record: ord-a74782c98fd94280bd383c6189f5da58
Source dataset: uspto-grants-2002_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06495576B2

Reaction notes

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